Preparation and standardisation of 0.1 M Titanium Trichloride using 0.1 M ferric ammonium sulphate and ammonium thiocyanate solution as indicator.
Titanium Trichloride Solution Preparation
- Dilute 100 ml of titanium trichloride solution with 200 ml of hydrochloric acid.
- Add sufficient freshly boiled and cooled water to produce 1000 ml.
Titanium Trichloride Solution Standardization
- Standardize the solution immediately before use by titrating with it in an atmosphere of carbon dioxide.
- Titrate 25 ml of 0.1 M ferric ammonium sulfate (acidified with sulphuric acid) with the 0.1 M Titanium Trichloride solution, using ammonium thiocyanate solution as indicator.
- 1 ml of 0.1 M ferric ammonium sulfate is equivalent to 0.01543 g of TiCl3.
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Dr. Ankur Choudhary is a prominent Pharmaceutical Quality Assurance expert, consultant and the founder of Pharmaguideline. With over 22 years of hands-on experience in cGMP-compliant manufacturing environments, he specializes in establishing validation protocols, sterile area controls and data integrity systems. Ankur routinely interprets international regulatory frameworks (including FDA, EMA and ICH guidelines) to help global pharmaceutical professionals ensure strict regulatory compliance and operational excellence. Connect with Ankur on LinkedIn. Need Help: Ask Question
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